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Beilstein J. Org. Chem. 2020, 16, 681–690, doi:10.3762/bjoc.16.66
Graphical Abstract
Figure 1: Structure of the target buckybowls 5a–c.
Scheme 1: Synthesis of dialkoxides 5a–c.
Scheme 2: Proposed mechanism of the formation of 5b and 5c.
Figure 2: Crystal structure of 5a. a) ORTEP drawing of the crystallographically independent unit with thermal...
Figure 3: a) Definition of POAV angle (φ). b) Side and c) top view of the molecular skeleton of 1. The double...
Figure 4: Crystal structure of 5b. a) ORTEP drawing of the crystallographically independent unit with thermal...
Figure 5: Crystal structure of 5c. a) ORTEP drawing of the crystallographically independent unit with thermal...
Figure 6: a) UV–vis spectra and b) emission spectra of 1 and dialkoxides 5a–c. For all the spectra, the conce...